Volume 8, Issue 1, March 2019, Page: 1-11
Structural, Optical and Magnetic Properties of (Ni, Al) Co-Doped ZnO Nanoparticles
Peyyala Swapna, Department of Physics, Sri Venkateswara University, Tirupati, India
Sakirevupalli Venkatramana Reddy, Department of Physics, Sri Venkateswara University, Tirupati, India
Received: Dec. 26, 2018;       Accepted: Jan. 21, 2019;       Published: Feb. 13, 2019
DOI: 10.11648/j.am.20190801.11      View  570      Downloads  139
We synthesize pure and (Ni, Al) co-doped Zinc Oxide (ZnO) nanoparticles by chemical co-precipitation method at room temperature successfully using poly ethylene glycol (PEG) as stabilizing agent. In the preparation, we kept one dopant element aluminum at constant concentration, 5 mol% by varying the other dopant concentration from one to three mol%. Following the completion of synthesis, the nanopowders are cautiously subjected to diverse characterizations such as XRD, SEM with EDS, TEM, PL, UV-Vis-NIR, Raman and VSM to determine the properties to be found the structural, optical and magnetic. XRD data shows that all the nanopowder samples acquire hexagonal wurtzite crystal structure by means of no secondary phases connecting to aluminum or nickel; this indicates the well dissolution of aluminum and nickel in to ZnO host lattice. The exact size of particles is predicted using TEM illustrations, which are more or less confirmed by the XRD data. The morphology of the samples is identified using SEM images, and EDS spectrum reveals that no impurities are present in the powder samples than nickel and aluminum. Optical properties are deliberated via PL spectrum and UV-Vis-NIR spectra, every one of the samples have defect related peaks in the visible region. Magnetic properties are estimated by means of the technique VSM, except pure ZnO nanoparticles remaining all the doped samples contains the Ferro magnetic nature.
Spintronics, Optoelectronics, DMS, Chemical Co-Precipitation, RTFM
To cite this article
Peyyala Swapna, Sakirevupalli Venkatramana Reddy, Structural, Optical and Magnetic Properties of (Ni, Al) Co-Doped ZnO Nanoparticles, Advances in Materials. Vol. 8, No. 1, 2019, pp. 1-11. doi: 10.11648/j.am.20190801.11
Copyright © 2019 Authors retain the copyright of this article.
This article is an open access article distributed under the Creative Commons Attribution License (http://creativecommons.org/licenses/by/4.0/) which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited.
A. Miyake, H. Kominami, H. Tatsuoka, H. Kuwabara, Y. Nakaushi and Y. Hatanaka, J. Cryst. Growth, 214 (2000)294-298.
J. Hu, T. W. Odom and C. M. Lieber, Acc. Chem. Res. 32 (1999) 435-445.
C. A. Mirkin, Science 286 (1999) 2095-2096.
S. M. Prokes and K. L. Wang, Mater. Res. Sci. Bull. 24 (1999) 13-19.
S. Nakamura, Science 281 (1998) 956-961.
M. Huang, S. Mao, H. Feick, H. Yan, Y. Wu, H. Kind, E. Weber, R. Russo and P. Yang, Science 292 (2001) 1897-1899.
E. Wong and P. Searson, Appl. phys. Lelt. 74 (1999 )2939-2941.
S. Choopun, R. Vvispute, W. Noch, A. Balsamo, R. Sharma, T. Venkatesan, A. Iliadis and D. Look, Appl. phys. Lelt. 75 (1999) 3947-3949.
A. sivagamsundari, R. Puzage, S. Chandra shekar, S. Ragagopan and R. Kannan, Appl. Nanosci. 3 (2013) 383-388.
D. Song, A. G. Aberle and J. Xia, Appl. Surf. Sci. 195 (2002) 291-296.
O. I. Lupan, S. T. Shishiyanu and T. S. Shishiyanu, Superlatt. Microstruct. 42 (2007) 375-378.
T. Dietl, H. Ohno, F. Matsukura, J. Cibert and D. Ferrand, Science 287 (2000) 1019-1022.
C. Karunakaran, V. Rajeswari and P. GomathiSankar, Super lattices Microstruc. 50 (2011) 234-241.
M. Nirmala, P. Smitha and A. Anukaliani, Super lattice Microstrure. 50 (2011) 563-571.
L Duan, W. Gao, R. Chen, Z. Fu, Solid state. Commu. 145 (2008) 479-481.
J. Yang, L. Feia, H. Liua, Y. Liu, M. Gaoa, Y. Zhanga and L. Yanga, J. Alloys Compd. 509 (2011) 3672-3676.
B. Sankara Reddy, S Venkatramana Reddy, P Venkateswara Reddy and N. Koteeswara Reddy Optoelectronics Adv. Mat. Rapid communications 6 (2012) 953-959.
P. Swapna and S. Venkatramana Reddy, Mechanics, Materials Science & Engineering, (2017) ISSN 2412-5954.
P Swapna and S Venkatramana Reddy, IOP Conf. Series: Materials Science and Engineering 310 (2018) 012011.
P Swapna and S Venkatramana Reddy, Adv. Sci. Lett. 24 (2018) 5636-5639.
A. Singhal, S. N Achary, J. Manjanna, S. Chatterjee, P. Ayyub and A. K. Tyagi, J. Phys. Chem. C 114 (2010) 3422-3430.
M. Schumm, M. Koerdel, S. Muller, C. Ronning, E. Dynowska, Z. Golacki, W. Szuszkiewicz and J. Geurts, Appl. Phys. 105 (2009) 083525.
P. Che, W. B. Liu, L. Guo, L. He and C. P. Chen, J. Magn. Magn. Mater. 320 (2008) 2563-2566.
B. Sankara Reddy, S. Venkatramana Reddy, N. Koteeswara Reddy J Mater Sci: Mater Electron 24 (2013) 5204-5210.
R. Wu, Y. Yang, S. Cong, Z. Wu, C. Xie, H. Usui, K. Kawaguchi and N. Koshizaki, Chemical Physics Letters406 (2005)457- 461.
M. Ghosh and AK. Raychaudhuri. Nanotechnology 19 (2008)445704.
R. Elilarassi, G. Chandrasekaran, J Mater sci: Mater Electron, springer science+Business media, (2010).
S. Muthukumaran, R. Gopalakrishnan, optical materials, Elsevier, (2012).
M. Kapilashrami, J. Xu, K. V. Rao and L. Belova, Processing and Application of Ceramics 4 (2010) 225-229.
J. Hu, Z. Zhang, Z. Zho, H. Qin and M. Jiang, Appl. Phys. Lett. 93 (2008) 192503.
M. Kapilashrami, J. Xu, V. Ström, K. V. Rao, L. Belova, Appl. Phys. Lett. 95 (2009) 033104.
Browse journals by subject